原花青素B1 标准品 Procyanidin B1,CAS:20315-25-7

产品编号 HYBP3023
产品分类 分析对照品、标准品
CAS号 20315-25-7
分子式 C30H26O12
分子量 578.52
品牌 华韵生物
规格 5mg
品牌 货号 纯度 规格 目录价(CNY) 会员价(CNY) 数量 购物车
华韵生物 HYBP3023-5mg HPLC≥98% 5mg ¥4000.00
CAS号 20315-25-7
分子式 C30H26O12
分子量 578.52
详情
CAS 20315-25-7
中文名称 原花青素B1
英文名称 Procyanidin B1
别名 Proanthocyanidin;
纯度 HPLC≥98%
分子式 C30H26O12
分子量 578.52
外观(性状) 白色至棕色粉末/White to brown Powder
保存 2-8℃
有效期 2 years
溶解性 ≥10mg/mL in DMSO
MDL MFCD01861512
SMILES O[C@H]1[C@@H](C2=CC=C(O)C(O)=C2)OC3=CC(O)=CC(O)=C3[C@@H]1C4=C5C(C[C@H](O)[C@@H](C6=CC=C(O)C(O)=C6)O5)=C(O)C=C4O
Note 储备液建议分装冻存,避免反复冻融(-20℃,1个月);稀释后的工作液建议现用现配/It is recommended to freeze the stock solution in several small portions to avoid repeated freezing and thawing (- 20 ℃, 1 month); The working solution is recommended to be used immediately after dilution
规格 5mg
单位

使用本产品的案例(仅供参考

UPLC-MS/MS

The analytical conditions were as follows, UPLC: column, C18 (1.8 μm, 2.1 mm × 100 mm); the mobile phase was consisted of solvent A, pure water with 0.1% formic acid, and solvent B, acetonitrile. Sample measurements were performed with a gradient program that employed the starting conditions of 95% A, 5% B. Within 9 min, a linear gradient to 5% A, 95% B was programmed, and a composition of 5% A, 95% B was kept for 1min. Subsequently, a composition of 95% A, 5.0% B was adjusted within 1.10 min and kept for 2.9 min. The column oven was set to 40 ◦C. The injection volume was 4 μL. 

The ESI source operation parameters were as follows: ion source, turbo spray; source temperature 550 ◦C; ion spray voltage (IS) 5500 V (positive ion mode)/-4500 V (negative ion mode); ion source gas I (GSI), gas II(GSII), curtain gas (CUR) were set at 50, 60, and 30.0 psi, respectively; the collision gas (CAD) was high. Instrument tuning and mass calibration were performed with 10 and 100 μM polypropylene glycol solutions in QQQ and LIT modes, respectively. QQQ scans were acquired as MRM experiments with collision gas (nitrogen) set to 5 psi. DP and CE for individual MRM transitions were done with further DP and CE optimization. A specific set of MRM transitions were monitored for each period according to the metabolites eluted within this period. 

来源文献:[1] Xiao Y , Li K , Zhang H ,et al.The profile of buckwheat tannins based on widely targeted metabolome analysis and pharmacokinetic study of ellagitannin metabolite urolithin A[J].LWT, 2022, 156:113069-.DOI:10.1016/j.lwt.2022.113069.


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